Eh-coupled release mechanisms of cadmium and arsenic in a contaminated paddy soil: An microcosm an synchrontron-based spectroscopic study

Liangdong Zhangaand J. Yanga b

aInstitute of Environment and Sustainable Development in Agriculture, Chinese Academy of Agricultural Sciences, China

bKey Laboratory of Agro-Environment, Ministry of Agriculture, China

liangdongz@qq.com

Cadmium (Cd) and arsenic (As) are identified as major contaminants in paddy fields, which was characteristic of frequently soil redox potential (Eh). However, Eh-coupled release mechanisms of Cd/As in contaminated paddy soils remains unclear. In this experiment, the combination of advanced microcosms and synchrotron-based X-ray fluorescence spectroscopy (μ-XRF) were applied to investigate the release mechanisms of As/Cd in the contaminated paddy soil at varied Eh conditions (-250, -50, 170 mV). The results indicated the concentrations of Cd, As, Al, S, P and Fe increased but DOC and pH decreased with the Eh increase from -250 mV to 170 mV. Cd/S/Al exhibited similar increasing pattern, with fast increase from -250 mV to -50 mV (Eh Range 1, EhR1), but slow increase from -50 mV to 170 mV (Eh Range 2, EhR2). However, As/Fe/P showed slow increase during EhR1 but fast increase during EhR2. Those suggested Cd and As were probably mainly correlated with sulfide oxidation and the reduction of Fe hydroxides during Eh changes, respectively. Moreover, μ-XRF analysis found As tended to overlap with Fe and S rather than K and Ca in the investigated soil for all Eh values, and the correlation coefficients of As-Fe and As-S were much higher at -250 mV and 170 mV compared to -50 mV. These results indicated As was probably associated with iron sulfide at low Eh condition but Fe hydroxides at high Eh condition. Collectively, iron sulfide was expected to be as the predominant sorbents for Cd/As sequestration at the low Eh condition, while the release of Cd was more sensitive to sulfide oxidation but that of As mainly depended on the reduction of Fe hydroxides with Eh changes from reducing to oxidation conditions. This study provides new insights on the co-release mechanisms of Cd/As in contaminated paddy soils, thus benefitting the control of rice contamination in paddy soils.

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